NurdRage | Lab Notes - Off the Shelf Catalyst Testing - Nov 11th 2018 @NurdRage | Uploaded 5 years ago | Updated 3 hours ago
We continue testing more catalysts for the sodium production reaction from magnesium and sodium hydroxide.

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#sodium

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$Make Wildfire (Trimethyl Borate) from Game of Thrones In this video we make Wildfire from Game of Thrones. Ive collaborated with my friend PixelLitch and sent him the bottle of wildfire which he used in his video here: https://www.youtube.com/watch?v=UkwaE0J5QFM The wildfire in this video is actually an azeotropic mixture of trimethyl borate and methanol. Trimethyl borate burns with an intense green flame that looks very much like wildfire from Game of Thrones. To make it we mix 200g of Borax, 650mL of methanol and 100g of sulfuric acid (98%). We then set up a fractional distillation column and distill of the fraction at 54 degrees Celsius which is azeotropic trimethyl borate. Glassware generously provided by http://www.alchemylabsupply.com/ Use the discount code copper for a 5% discount. Donate to NurdRage! Through Patreon (preferred): https://www.patreon.com/NurdRage Through Bitcoin: 1NurdRAge7PNR4ULrbrpcYvc9RC4LDp9pS This video generously supported by: Only HR advisable Michael Zappe Emil Mikulic Alex S. Phillip Hutchings Cullen Purkis Simon Bitdiddle Samuel Pelzer Matthew Brunette Meshal Al-Enazi Lord Martin Hill Max Loutzenheiser Carl Potter LVE Wesley Gardner Jack kelly Collin Wright$

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$Make Chlorotoluene (mixture of isomers) 1st step in making Pyrimethamine Glassware generously provided by http://www.alchemylabsupply.com/ Use the discount code copper for a 5% discount. Donate to NurdRage! Through Patreon (preferred): https://www.patreon.com/NurdRage Video on popchest: https://video.popchest.com/video/1652 How to make chlorine gas: https://www.youtube.com/watch?v=hLHfN7GvAyI Fractional distillation of lacquer thinner to obtain toluene: https://www.youtube.com/watch?v=ddCuWX4vtOA In this video we demonstrate the synthesis of chlorotoluenes. In the first process we react 4 moles of chlorine (2 moles of chlorine gas) with 500mL of toluene and 10g of steel wool in a flask with a reflux condenser. We then remove the steel wool and wash the chlorotoluenes with water and a saturated solution of sodium bicarbonate. Then we fractionally distill the organic layer to obtain chlorotoluenes in the boiling range of 135-170 Celsius. In the second process we mix 125g of anhydrous ferrous chloride and 500mL of toluene. With vigorous stirring we add a total 160g of trichloroisocyanuric acid by 10g every 15 minutes or slower if the reaction begins to reflux. After the last addition the mixture is stirred overnight and then the organics are recovered using a dean stark trap and 500mL of water as the carrier solvent. The organic layer is then fractionally distilled to obtain chlorotoluenes as before. This video was generously sponsored by: Robert Boll Brian Empson Kevin S Only HR Scott Malcheski advisable Michael Zappe Emil Mikulic Dino Capiaghi Benjamin Nied Wesley Gardner LVE Meshal Al-Enazi Lord Martin Hill Matthew Brunette Collin Wright Simon Bitdiddle Cullen Purkis Samuel Pelzer Carl Potter Max Loutzenheiser Jack kelly Phillip Hutchings$

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Lab Notes - Off the Shelf Catalyst Testing - Nov 11th 2018 @NurdRage